高分辨NH3光谱检测的气压控制系统设计
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1.中国科学院环境光学与技术重点实验室 中国科学院合肥物质科学研究院,安徽 合肥 230031; 2.中国科学技术大学,安徽 合肥 23002

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TP273

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国家自然科学基金青年项目(41805124)、安徽省重点研究和开发计划(201904a07020093)、中科院科研仪器设备研制项目(YJKYYQ20190051)资助


Design of air pressure control system for high resolution NH3 spectrum detection
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1.Key Laboratory of Environmental Optics& Technology, Chinese Academy of Sciences, Hefei Institute of Material Science, Chinese Academy of Sciences, Hefei 230031, Anhui, China; 2.University of Science and Technology of China, Hefei, 230026, Anhui, China

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    摘要:

    本文基于伯努利原理设计了被测氨气气压闭环反馈控制系统,研究了低压条件下NH3高分辨光谱特性。系统以被测氨气吸收池压力为控制对象,采用CDG800压力传感器测量吸收池气压,1路VT317电磁阀控制高压标准浓度氨气源增大吸收池中的气压,1路VT317电磁阀控制真空泵抽取吸收池的气体降低气压,构成了NH3光谱检测的低压气路;并设计以Arduino UNO单片机为核心的压力测量、电磁阀和真空泵闭环反馈控制电路。实验结果显示,设计的气压控制系统可维持稳定时间达72小时以上,气压波动在1torr以内;压力为3.2torr时获得了NH3中红外波段1103.4cm-1的六条单根吸收光谱信号,计算得到的线强与HITRAN数据库中线强数据偏差约在2.71%-4.71%之间,实现了重叠谱线完全分离,为后续的高分辨光谱研究提供了宝贵经验。

    Abstract:

    In this paper, a closed-loop feedback control system for the measured ammonia gas pressure is designed based on Bernoulli's principle, and the high-resolution spectral characteristics of NH3 under low pressure conditions are studied. The system takes the measured ammonia absorption tank pressure as the control object, uses CDG800 pressure sensor to measure the absorption tank air pressure, one of the VT317 solenoid valve controls the high pressure standard concentration ammonia source to increase the air pressure in the absorption tank, and the other VT317 solenoid valve controls the vacuum pump extraction The gas in the absorption cell reduces the pressure to form a low-pressure gas circuit for NH3 spectrum detection; and a closed-loop feedback control circuit for pressure measurement, solenoid valve and vacuum pump with Arduino UNO microcontroller as the core is designed. The experimental results show that the designed air pressure control system can maintain a stable time for more than 72 hours, and the air pressure fluctuates within 1 torr. A single absorption spectrum signal in the NH3 mid-infrared band 1103.4cm-1 is obtained, and the calculated line intensity is consistent with the center line of the HITRAN database. The strong data deviation is between 2.71% and 4.71%.

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李梦琪,张玉钧,何莹,尤坤,王立明.高分辨NH3光谱检测的气压控制系统设计[J].电子测量技术,2021,44(2):36-42

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  • 在线发布日期: 2024-12-19
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